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Collect. Czech. Chem. Commun. 1984, 49, 1605-1616
https://doi.org/10.1135/cccc19841605

Assignment of 1H and 13C NMR spectra by a combination of homo- and heteronuclear shift correlated two-dimensional NMR. Application to oligosaccharides related to arabinoxylane

Jan Schramla, Ján Hirschb, Eva Petrákováb, Eduard Krahéc and Claus Bliefertc

a Institute of Chemical Process Fundamentals, Czechoslovak Academy of Sciences, 165 02 Prague, ČSSR
b Institute of Chemistry, Slovak Academy of Sciences, 842 38 Bratislava, ČSSR
c Fachhochschule Munster, Fachbereich Chemieingenieurwesen, D-4430 Steinfurt 1, FGR

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  • Teleman Anita, Harjunpää Vesa, Tenkanen Maija, Buchert Johanna, Hausalo Tiina, Drakenberg Torbjörn, Vuorinen Tapani: Characterisation of 4-deoxy-β-l-threo-hex-4-enopyranosyluronic acid attached to xylan in pine kraft pulp and pulping liquor by 1H and 13C NMR spectroscopy. Carbohydrate Research 1995, 272, 55. <https://doi.org/10.1016/0008-6215(95)96873-M>
  • Harket Mouna, De Jeso Bernard, Lartigue Jean-Claude, Petraud Michel, Ratier Max: Application of the 29Si NMR 2D INEPT spin-flip J-resolved technique to the structural analysis of trimethylsilylated glycosides. Carbohydrate Research 1994, 263, 155. <https://doi.org/10.1016/0008-6215(94)00163-4>
  • Šimkovic Ivan, Antal Miroslav, Alföldi Juraj: Fractionation of wheat straw meal after pretreatment with acidified zinc chloride solutions. Carbohyd Polymers 1994, 23, 111. <https://doi.org/10.1016/0144-8617(94)90034-5>
  • Bock Klaus, Duus Jens Ø., Norman Barrie, Pedersen Sven: Assignment of structures to oligosaccharides produced by enzymic degradation of a β-d-glucan from barley by 1H- and 13C-n.m.r. spectroscopy. Carbohydrate Research 1991, 211, 219. <https://doi.org/10.1016/0008-6215(91)80093-3>
  • Ebringerová Anna, Hromádková Zdenka, Petráková Eva, Hricovíni Miloš: Structural features of a water-soluble l-arabino-d-xylan from rye bran. Carbohydrate Research 1990, 198, 57. <https://doi.org/10.1016/0008-6215(90)84276-Z>
  • Schraml J., Petráková E., Hirsch J.: 29Si and 13C NMR spectra of all possible pertrimethylsilylated β‐D‐xylopyranosyl‐substituted methyl 4‐O‐β‐D‐xylopyranosyl‐β‐D‐xylopyranosides assigned by 2D heteronuclear 1H‐29Si and 1H‐13C chemical shift correlations. Magnetic Reson in Chemistry 1987, 25, 75. <https://doi.org/10.1002/mrc.1260250118>
  • Brillouet Jean-Marc, Joseleau Jean-Paul: Investigation of the structure of a heteroxylan from the outer pericarp (beeswing bran) of wheat kernel. Carbohydrate Research 1987, 159, 109. <https://doi.org/10.1016/S0008-6215(00)90009-0>
  • Šimkovic Ivan, Alföldi Juraj, Matulová Mária: A 13C-n.m.r. study of the alkaline degradation products of polysaccharides. Carbohydrate Research 1986, 152, 137. <https://doi.org/10.1016/S0008-6215(00)90294-5>
  • Schramla Jan, Petráková Eva, Pelnař Jan, Kvíačlova Magdalena, Chvalovský Václav: Trimethylsilylation - Aid in NMR Analysis of Oligosaccharides. Assigment of 29Si and 13C NMR Spectra of Trimethylsilylated Methyl β-D-Xylobiosides by 2D NMR. Journal of Carbohydrate Chemistry 1985, 4, 393. <https://doi.org/10.1080/07328308508070189>